1Adopting standards:
GB/T 214-2007 "Method for determination of total sulfur in coal"
GB/T 483-2007 General Provisions for Coal Analysis Experimental Methods
GB/T 387-1990 "Determination of sulfur content in dark petroleum products - Tube furnace method"
II Scope of application:
Suitable for the determination of total sulfur in materials such as lignite, bituminous coal, anthracite, coke, dry coal samples of coal water slurry, and heavy oil in industries such as electricity, coal mining, metallurgy, chemical engineering, cement, geological exploration, and scientific research institutions.
IIITechnical parameters:
1Measurement range of sulfur:0-10%The resolution is:0.001%.
2Sample combustion analysis time: approximately after startup500Staying at ℃45Perform pre decomposition in seconds and then automatically advance to1050℃ position.5Automatically determine whether the experiment has ended and returned in about minutes, the longest time8minute.
3Temperature measurement and control accuracy:1050±5℃
4High temperature furnace: working temperature ≤1200℃, constant temperature zone length ≥90mmThe heating element is a double threaded silicon carbon tube (model: φ)40/30×400)Under program control30About minutes to reach1050℃.
5Electrolytic cell: with a volume of400mlThe electrode material is platinum, and the specifications of the electrolytic electrode are10mm×15mmIndicating electrode specifications:5mm×10mmElectrolyte volume: approximately260ml.
6Instrument measurement accuracy: superior toGB214-2007The requirements.
7Power supply:AC220V±10%,50Hz, ≤10A.
8Environmental temperature:5~40℃;
9Relative humidity:≤85%;
10Installation environmentThere should be no strong air convection or corrosive gases indoors, and it should be kept away from strong electromagnetic field equipment as much as possible. It should not share the same phase power supply with other high-power electrical equipment.
11SampleParticle size less than0.2mm, weighing once50mg±2mg, accurate to0.1mg.
12Instrument size(mm)Controller:364(long)×364(wide)×170(tall)
High temperature furnace:560(long)×250(wide)×270(tall)
4Performance characteristics:
1The human-machine interface is friendly, with a large touch screen displaying Chinese characters and Chinese voice. Highly intelligent, the entire experimental process is intelligently controlled by the program, and users only need to input the sample weight and wait for about five minutes to obtain the test data.
2Optimized heating program, adoptingPIDThe mode control of furnace flow not only expands the selection range of resistance values for silicon carbon tubes, but also fully protects them, significantly extending their service life.
3The sample delivery mechanism adopts electronic travel switches, magnetic Hall devices, and non-contact sensing of the sample delivery position.
4The instrument automatically determines the endpoint of the titration test and exits in a timely manner, accompanied by a buzzing prompt, to improve work efficiency.
5Allow users to make overall or segmented corrections for measurement deviations caused by testing conditions, with built-in overall coefficient calculation function, automatically stored after calculation, and simple and easy error correction.
6Input and analyze moisture values to calculate the sulfur content on a dry basis for printing.
7Real time display of furnace temperature, furnace flow, process time, sulfur content during the experiment, and sample weight can be modified at any time before the end of the experiment.
8Can power down and remember the latest information32A historical record can be printed using the reprint function
